Technology Process of C17H20ClNO5
There total 1 articles about C17H20ClNO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on carbon; hydrogen;
In
tetrahydrofuran;
at 23 ℃;
for 12h;
optical yield given as %de;
DOI:10.1021/jo101638r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere
2.1: n-butyllithium; zinc(II) chloride / Inert atmosphere
2.2: Inert atmosphere
3.1: ammonium cerium (IV) nitrate; water / methanol / 6 h / 0 °C / Inert atmosphere
With
dichloro-acetic acid; n-butyllithium; ammonium cerium (IV) nitrate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride;
In
methanol; dimethyl sulfoxide; toluene;
1.1: Moffatt oxidation;
DOI:10.1021/jo101638r
- Guidance literature:
-
With
dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dimethyl sulfoxide; toluene;
at 23 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/jo101638r