(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

Base Information

Chemical Name:(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane
CAS No.:289889-74-3
Molecular Formula:C₂₃H₂₈F₃NO₃
Molecular Weight:423.475
Hs Code.:

Synonyms:(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

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Chemical Property of (+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

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Technology Process of (+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

There total 3 articles about (+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 289889-72-1
(+/-)-N-trifluoroacetyl-1-[2,5-dimethoxy-4-(4-phenyl-1-butynyl)phenyl]-2-aminopropane

: 289889-74-3
(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h; under 2068.59 Torr;
DOI:10.1021/jm9906062

Reference yield:

: 111381-04-5
N-trifluoroacetyl-1-(2,5-dimethoxy-4-iodophenyl)-2-aminopropane

: 289889-74-3
(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / pyridine / 120 °C

2: 46 percent / H₂ / 10 percent Pd/C / methanol / 4 h / 2068.59 Torr

With pyridine; hydrogen; palladium on activated charcoal; In methanol; 1: Substitution / 2: Catalytic hydrogenation;
DOI:10.1021/jm9906062

Reference yield:

: (4-phenylbut-1-yn-1-yl)copper

: 289889-74-3
(+/-)-N-trifluoro-2-[2,5-dimethoxy-4-(4-phenylbutyl)phenyl]-2-aminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / pyridine / 120 °C

2: 46 percent / H₂ / 10 percent Pd/C / methanol / 4 h / 2068.59 Torr

With pyridine; hydrogen; palladium on activated charcoal; In methanol; 1: Substitution / 2: Catalytic hydrogenation;
DOI:10.1021/jm9906062