tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

Base Information

Chemical Name:tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate
CAS No.:1229245-15-1
Molecular Formula:C₂₃H₃₃NO₄
Molecular Weight:387.519
Hs Code.:

Synonyms:tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

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Chemical Property of tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

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Technology Process of tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

There total 6 articles about tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-16-2
tert-butyl cyclopropyl(3,5-dibromobenzyl)carbamate

: 165059-42-7,934342-48-0
(E)-3-methoxy-1-propenylboronic acid pinacol ester

: 1229245-15-1
tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

Guidance literature:: With sodium carbonate; trans-dichlorobis(triphenylphosphine)palladium(II); In water; N,N-dimethyl-formamide; at 90 ℃; for 6h; Inert atmosphere of nitrogen;

Reference yield:

: 1229245-17-3
N-[(3,5-dibromophenyl)methyl]cyclopropanamine

: 1229245-15-1
tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

2: sodium carbonate / trans-dichlorobis(triphenylphosphine)palladium(II) / water; N,N-dimethyl-formamide / 6 h / 90 °C / Inert atmosphere of nitrogen

With sodium carbonate; N-ethyl-N,N-diisopropylamine; trans-dichlorobis(triphenylphosphine)palladium(II); In dichloromethane; water; N,N-dimethyl-formamide; 2: Suzuki Coupling;

Reference yield:

: C₁₀H₉Br₂N

: 1229245-15-1
tert-butyl {3,5-bis[(1E)-3-methoxy-1-propen-1-yl]benzyl}cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

3: sodium carbonate / trans-dichlorobis(triphenylphosphine)palladium(II) / water; N,N-dimethyl-formamide / 6 h / 90 °C / Inert atmosphere of nitrogen

With sodium tetrahydroborate; sodium carbonate; N-ethyl-N,N-diisopropylamine; trans-dichlorobis(triphenylphosphine)palladium(II); In methanol; dichloromethane; water; N,N-dimethyl-formamide; 3: Suzuki Coupling;