Technology Process of C54H76N4O16S2
There total 8 articles about C54H76N4O16S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; trifluoroacetic acid;
In
dichloromethane;
at 0 ℃;
for 4h;
DOI:10.1002/chem.201000611
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: silver(l) oxide / dichloromethane / 48 h / 20 °C
2.1: sodium azide / ethanol / 8 h / Reflux
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h
4.2: 20 °C
5.1: triphenylphosphine / tetrahydrofuran / 8 h / 20 °C
5.2: 48 h
6.1: triethylamine / dichloromethane / 20 °C
7.1: sodium hydride / tetrahydrofuran / 0.17 h
7.2: 20 °C
8.1: water; trifluoroacetic acid / dichloromethane / 4 h / 0 °C
With
sodium azide; water; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; silver(l) oxide;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
4.1: Williamson reaction / 4.2: Williamson reaction / 5.1: Staudinger reaction / 5.2: Staudinger reaction;
DOI:10.1002/chem.201000611
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triphenylphosphine / tetrahydrofuran / 8 h / 20 °C
1.2: 48 h
2.1: triethylamine / dichloromethane / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.17 h
3.2: 20 °C
4.1: water; trifluoroacetic acid / dichloromethane / 4 h / 0 °C
With
water; sodium hydride; triethylamine; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
1.1: Staudinger reaction / 1.2: Staudinger reaction;
DOI:10.1002/chem.201000611
