Cp(PMe₂Ph)2RuSiCl₃

Base Information

Chemical Name:Cp(PMe₂Ph)2RuSiCl₃
CAS No.:475635-23-5
Molecular Formula:C₂₁H₂₇Cl₃P₂RuSi
Molecular Weight:576.907
Hs Code.:

Cp(PMe<sub>2</sub>Ph)2RuSiCl<sub>3</sub>

Synonyms:Cp(PMe₂Ph)2RuSiCl₃

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Chemical Property of Cp(PMe₂Ph)2RuSiCl₃

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Technology Process of Cp(PMe₂Ph)2RuSiCl₃

There total 1 articles about Cp(PMe₂Ph)2RuSiCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.2%

: 10026-04-7,53609-55-5
tetrachlorosilane

: 310896-06-1
Ru(C₅H₅)H(P(CH₃)2C₆H₅)2

: 475635-23-5
Cp(PMe₂Ph)2RuSiCl₃

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; byproducts: 1,8-diazabicyclo[5.4.0]undec-7-enium chloride; (Ar); addn. of silicon compd. to a frozen soln. of ruthenium complex andDBU in CH2Cl2, warming to room temp., stirring for 1.5 h; evapn., extn. with Et2O, filtration through Celite, concn., addn. of hexanes, concn., filtration, drying in vac.; elem. anal.;
DOI:10.1021/om0204235

Reference yield: 76.0%

: 475635-23-5
Cp(PMe₂Ph)2RuSiCl₃

: 75-24-1
trimethylaluminum

: 475635-31-5
C₅H₅Ru(PC₆H₅(CH₃)2)2Si(CH₃)3

Guidance literature:: In toluene; (Ar); addn. of aluminum compd. to a suspn. of ruthenium complex in toluene, stirring at room temp. for 1 h; evapn., extn. with hexanes, filtration through Celite, evapn., extn. with hexanes, filtration through Celite, evapn.; elem. anal.;
DOI:10.1021/om0204235

Reference yield: 75.0%

: 16853-85-3
lithium aluminium tetrahydride

: 475635-23-5
Cp(PMe₂Ph)2RuSiCl₃

: 475635-29-1
C₅H₅Ru(PC₆H₅(CH₃)2)2SiH₃

Guidance literature:: In diethyl ether; (Ar); addn. of Et2O to a mixt. of ruthenium complex and LiAlH4, stirringfor 1.5 h at room temp.; evapn., extn. with hexanes, filtration through Celite, evapn., elem. anal.;
DOI:10.1021/om0204235