C₄₀H₄₈Cl₃NO₁₂Si

Base Information

Chemical Name:C₄₀H₄₈Cl₃NO₁₂Si
CAS No.:1415724-88-7
Molecular Formula:C₄₀H₄₈Cl₃NO₁₂Si
Molecular Weight:869.265
Hs Code.:

C<sub>40</sub>H<sub>48</sub>Cl<sub>3</sub>NO<sub>12</sub>Si

Synonyms:C₄₀H₄₈Cl₃NO₁₂Si

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Chemical Property of C₄₀H₄₈Cl₃NO₁₂Si

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Technology Process of C₄₀H₄₈Cl₃NO₁₂Si

There total 4 articles about C₄₀H₄₈Cl₃NO₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1415724-87-6
C₄₄H₅₂Cl₃NO₁₄Si

: 1415724-88-7
C₄₀H₄₈Cl₃NO₁₂Si

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at -20 ℃; for 36h;
DOI:10.1021/ol303122w

Reference yield:

: 273400-74-1
phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

: 1415724-88-7
C₄₀H₄₈Cl₃NO₁₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylsilane / dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 1 h / -20 °C / Molecular sieve; Inert atmosphere

2.1: dmap / pyridine / 12 h / 20 °C / Inert atmosphere

3.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 1 h / 0 °C / Molecular sieve; Inert atmosphere

4.1: sodium methylate; methanol / tetrahydrofuran / 36 h / -20 °C

With methanol; triethylsilane; dmap; sodium methylate; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/ol303122w

Reference yield:

: C₂₁H₂₂Cl₃NO₅S

: 1415724-88-7
C₄₀H₄₈Cl₃NO₁₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / pyridine / 12 h / 20 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 1 h / 0 °C / Molecular sieve; Inert atmosphere

3.1: sodium methylate; methanol / tetrahydrofuran / 36 h / -20 °C

With methanol; dmap; sodium methylate; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/ol303122w