phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside
CAS No.:273400-74-1
Molecular Formula:C₂₁H₂₀Cl₃NO₅S
Molecular Weight:504.818
Hs Code.:

Synonyms:phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Suppliers and Price of phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

There total 2 articles about phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: phenyl 2-deoxy-1-thio-2-trichloroacetamido-β-D-galactopyranoside

: 273400-74-1
phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2013.10.011

Reference yield:

: 198200-67-8
phenyl 3,4,6-tri-O-acetyl-2-deoxy-1-thio-2-trichloroacetamido-β-D-galactopyranoside

: 273400-74-1
phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

2: camphor-10-sulfonic acid / acetonitrile / 16 h / Inert atmosphere

With camphor-10-sulfonic acid; sodium methylate; In methanol; acetonitrile;
DOI:10.1016/j.tet.2013.10.011

Reference yield: 90.0%

: 273400-74-1
phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

: 123-76-2
levulinic acid

: phenyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-1-thio-β-D-galactopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2013.10.011