7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

Base Information

Chemical Name:7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine
CAS No.:902452-70-4
Molecular Formula:C₂₂H₂₅N₅O₆
Molecular Weight:455.47
Hs Code.:

Synonyms:7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

Chemical Property:

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Technology Process of 7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

There total 5 articles about 7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 902452-69-1
7-(5-O-benzoyl-3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

: 902452-70-4
7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

Guidance literature:: With pyridine; sodium hydroxide; In ethanol; water;
DOI:10.1016/j.tet.2006.04.016

Reference yield:

: 902452-68-0
7-(2-O-acetyl-3-O-benzyl-4-C-methanesulfonyloxy-5-O-methanesulfonyl-β-D-erythro-pentofuranosyl)-2-N-isobutyrylguanine

: 902452-70-4
7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaOH / dioxane; H₂O

2: 93 percent / dimethylformamide

3: 85 percent / NaOH; pyridine / ethanol; H₂O

With pyridine; sodium hydroxide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.04.016

Reference yield:

: 21047-89-2
2-N-isobutyrylguanine

: 902452-70-4
7-(3-O-benzyl-2-O,4-C-methylene-β-D-ribofuranosyl)-2-N-isobutyrylguanine

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile

1.2: 34 percent / SnCl₄ / acetonitrile / 20 h

2.1: 89 percent / NaOH / dioxane; H₂O

3.1: 93 percent / dimethylformamide

4.1: 85 percent / NaOH; pyridine / ethanol; H₂O

With pyridine; sodium hydroxide; N,O-bis-(trimethylsilyl)-acetamide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2006.04.016