C₃₈H₄₈N₄O₈S

Base Information

Chemical Name:C₃₈H₄₈N₄O₈S
CAS No.:1029259-59-3
Molecular Formula:C₃₈H₄₈N₄O₈S
Molecular Weight:720.887
Hs Code.:

C<sub>38</sub>H<sub>48</sub>N<sub>4</sub>O<sub>8</sub>S

Synonyms:C₃₈H₄₈N₄O₈S

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Chemical Property of C₃₈H₄₈N₄O₈S

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Technology Process of C₃₈H₄₈N₄O₈S

There total 15 articles about C₃₈H₄₈N₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1029259-73-1
tert-butyl (6S,13aS,14aR,16aS,Z)-14a-(cyclopropylsulfonylcarbamoyl)-2,5,16-trioxo-1,2,3,5,6,7,8,9,10,11,13a,14,14a,15,16,16a-hexadecahydrocyclopropa[e]pyrrolo[1,2-a][1,4]diazacyclopentadecin-6-ylcarbamate

: 1201-71-4
4-biphenyllithium

: 1029259-59-3
C₃₈H₄₈N₄O₈S

Guidance literature:: tert-butyl (6S,13aS,14aR,16aS,Z)-14a-(cyclopropylsulfonylcarbamoyl)-2,5,16-trioxo-1,2,3,5,6,7,8,9,10,11,13a,14,14a,15,16,16a-hexadecahydrocyclopropa[e]pyrrolo[1,2-a][1,4]diazacyclopentadecin-6-ylcarbamate; With MgBr₂*Et₂O; In tetrahydrofuran; at 0 - 20 ℃;

4-biphenyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 3h;

With ammonium chloride; In tetrahydrofuran; hexane; water;

Reference yield:

: 40216-83-9
L-4-hydroxyproline methyl ester hydrochloride

: 1029259-59-3
C₃₈H₄₈N₄O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: 4-methyl-morpholine; HATU / dichloromethane / 72 h / 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 16 h / 20 °C

2.2: pH 4

3.1: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 16 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C

5.1: tri(cycloxexyl)phosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene][benzylidene]ruthenium(IV) dichloride / dichloromethane / 0.25 h / Heating / reflux

6.1: lithium hydroxide; water / tetrahydrofuran; methanol / 4 h / 20 °C

6.2: pH 4

7.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Heating / reflux

7.2: 4 h / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

9.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

10.1: MgBr₂*Et₂O / tetrahydrofuran / 0 - 20 °C

10.2: 3 h / -78 - 0 °C

With 4-methyl-morpholine; 1H-imidazole; lithium hydroxide; MgBr₂*Et₂O; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; HATU; 1,1'-carbonyldiimidazole; tri(cycloxexyl)phosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene][benzylidene]ruthenium(IV) dichloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 213316-32-6,259221-73-3
rac-(1R,2S)-1-amino-2-vinylcyclopropanecarboxylic acid ethyl ester

: 1029259-59-3
C₃₈H₄₈N₄O₈S

Guidance literature:: Multi-step reaction with 11 steps

1.1: tert-butyl methyl ether; toluene / 20 °C / Heating / reflux

2.1: esperase 8.0L / water; dimethyl sulfoxide / 90 h / 40 °C / pH 8.5 / Heps*Na buffer; Enzymatic reaction; Resolution of racemate

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

4.1: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide / 16 h / 20 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C

6.1: tri(cycloxexyl)phosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene][benzylidene]ruthenium(IV) dichloride / dichloromethane / 0.25 h / Heating / reflux

7.1: lithium hydroxide; water / tetrahydrofuran; methanol / 4 h / 20 °C

7.2: pH 4

8.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Heating / reflux

8.2: 4 h / 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

10.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

11.1: MgBr₂*Et₂O / tetrahydrofuran / 0 - 20 °C

11.2: 3 h / -78 - 0 °C

With 4-methyl-morpholine; 1H-imidazole; hydrogenchloride; lithium hydroxide; esperase 8.0L; MgBr₂*Et₂O; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; HATU; 1,1'-carbonyldiimidazole; tri(cycloxexyl)phosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene][benzylidene]ruthenium(IV) dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; tert-butyl methyl ether; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;