Cyclopropanecarboxylic acid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride (1:1),(1R,2S)-rel-

Base Information

• Chemical Name: Cyclopropanecarboxylic acid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride (1:1),(1R,2S)-rel-
• CAS No.: 259214-54-5
• Molecular Formula: C₈H₁₃NO₂*ClH
• Molecular Weight: 191.658
• Mol file: 259214-54-5.mol

Synonyms:Cyclopropanecarboxylicacid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride, (1R,2S)-rel- (9CI)

Chemical Property of Cyclopropanecarboxylic acid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride (1:1),(1R,2S)-rel-

Chemical Property:

• PSA: 52.32000
• LogP: 1.95520

Purity/Quality:

97% ^*data from raw suppliers

Cyclopropanecarboxylicacid,1-amino-2-ethenyl-,ethylester,hydrochloride(1:1),(1R,2S)-rel- 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxylic acid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride (1:1),(1R,2S)-rel-

There total 24 articles about Cyclopropanecarboxylic acid, 1-amino-2-ethenyl-, ethyl ester, hydrochloride (1:1),(1R,2S)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(1R,2S)-ethyl 1-(tert-butoxycarbonylamino)-2-vinylcyclopropanecarboxylate (681807-59-0,213316-49-5) → (1R,2S)-ethyl 1-amino-2-vinylcyclopropanecarboxylate hydrochloride (681807-60-3,259214-54-5,259214-56-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

Reference yield: 100.0%

(1RS,2SR)-ethyl 2-vinyl-1-(tert-butoxycarbonylamino)cyclopropanecarboxylate (213316-49-5) → (trans)-ethyl 1-amino-2-vinylcyclopropanecarboxylate hydrochloride (259214-54-5,259214-56-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h; Product distribution / selectivity;

Reference yield: 100.0%

N-Boc-(1R,2S)-1-amino-2-vinylcyclopropane carboxylic acid ethyl ester (259217-95-3,213316-49-5) → ethyl (1R,2S)-1-amino-2-vinylcyclopropanecarboxylate hydrochloride (259214-54-5,259214-56-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

upstream raw materials:

N-Boc-(1R,2S)-1-amino-2-vinylcyclopropane carboxylic acid ethyl ester

(1S,2R)-ethyl 2-vinyl-1-(tert-butoxycarbonylamino)cyclopropanecarboxylate

(1R,2S)-ethyl 1-(tert-butoxycarbonylamino)-2-vinylcyclopropanecarboxylate

rac-(1R,2S)-1-amino-2-vinylcyclopropanecarboxylic acid ethyl ester

Downstream raw materials:

(2S,4R)-tert-butyl 2-((1R,2S)-1-(ethoxycarbonyl)-2-vinylcyclopropylcarbamoyl)-4-hydroxypyrrolidine-1-carboxylate

(1R,2S)-1-{[(1R,2R,4S)-2-(hex-5-enyl-methyl-carbamoyl)-4-hydroxy-cyclopentanecarbonyl]-amino}-2-vinyl-cyclopropanecarboxylic acid ethyl ester

(1R,2S)-ethyl 1-((2S,4R)-1-((S)-2-(((tert-butoxy)carbonyl)amino)non-8-enoyl)-4-hydroxypyrrolidine-2-carboxamido)-2-vinylcyclopropanecarboxylate

C₃₂H₄₄N₄O₈S

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