2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

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Chemical Name:2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate
CAS No.:1379764-25-6
Molecular Formula:C₂₇H₂₃N₂O₃S₂*ClO₄
Molecular Weight:587.074
Hs Code.:

Synonyms:2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

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Chemical Property of 2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

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Technology Process of 2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

There total 2 articles about 2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1379764-13-2
2-(methoxycarbonyl)-9-phenylthieno[2,3-b]quinolinium perchlorate

: 332345-27-4
5-(4-morpholinyl)thiophene-2-carboxylic acid

: 1379764-25-6
2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

Guidance literature:: With acetic anhydride; for 4h; Reflux;
DOI:10.3998/ark.5550190.0013.325

Reference yield:

: 313352-89-5
methyl 2-(N,N-diphenylamino)thiophene-5-carboxylate

: 1379764-25-6
2-methoxycarbonyl-4-[5-(N-morpholinyl)-2-thienyl]-9-phenylthieno[2,3-b]quinolinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.33 h / 60 °C / Cooling

1.2: Cooling

2.1: acetic anhydride / 4 h / Reflux

With acetic anhydride; trichlorophosphate;
DOI:10.3998/ark.5550190.0013.325