C₄₈H₄₈O₈P₂

Base Information

Chemical Name:C₄₈H₄₈O₈P₂
CAS No.:1356412-08-2
Molecular Formula:C₄₈H₄₈O₈P₂
Molecular Weight:814.852
Hs Code.:

C<sub>48</sub>H<sub>48</sub>O<sub>8</sub>P<sub>2</sub>

Synonyms:C₄₈H₄₈O₈P₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₄₈O₈P₂

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Technology Process of C₄₈H₄₈O₈P₂

There total 13 articles about C₄₈H₄₈O₈P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1356412-06-0
C₄₈H₄₈O₁₀P₂

: 1356412-08-2
C₄₈H₄₈O₈P₂

Guidance literature:: With tributyl-amine; trichlorosilane; In 5,5-dimethyl-1,3-cyclohexadiene; at 10 - 130 ℃; for 5.25h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.11.111

Reference yield:

: 1356412-03-7
[2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-7-yl]diphenylphosphine

: 1356412-08-2
C₄₈H₄₈O₈P₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: dihydrogen peroxide / methanol; water / 2.5 h / 15 - 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 3.5 h / -70 °C / Inert atmosphere

2.2: -70 - 20 °C / Inert atmosphere

3.1: copper / N,N-dimethyl-formamide / 12 h / 150 °C / Inert atmosphere

4.1: tributyl-amine; trichlorosilane / 5,5-dimethyl-1,3-cyclohexadiene / 5.25 h / 10 - 130 °C / Inert atmosphere

With tributyl-amine; trichlorosilane; dihydrogen peroxide; copper; lithium diisopropyl amide; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide; 3.1: Ullmann reaction;
DOI:10.1016/j.tetlet.2011.11.111

Reference yield:

: 1356411-94-3
(2R,3R)-2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-6-amine

: 1356412-08-2
C₄₈H₄₈O₈P₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; sodium nitrite / water; acetonitrile / 0.5 h / 0 - 5 °C / Inert atmosphere

1.2: 1 h / 55 - 60 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -75 °C / Inert atmosphere

2.2: 3.75 h / -75 - 0 °C / Inert atmosphere

3.1: dihydrogen peroxide / methanol; water / 2.5 h / 15 - 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 3.5 h / -70 °C / Inert atmosphere

4.2: -70 - 20 °C / Inert atmosphere

5.1: copper / N,N-dimethyl-formamide / 12 h / 150 °C / Inert atmosphere

6.1: tributyl-amine; trichlorosilane / 5,5-dimethyl-1,3-cyclohexadiene / 5.25 h / 10 - 130 °C / Inert atmosphere

With n-butyllithium; tributyl-amine; trichlorosilane; dihydrogen peroxide; copper; acetic acid; lithium diisopropyl amide; sodium nitrite; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; hexane; water; N,N-dimethyl-formamide; acetonitrile; 5.1: Ullmann reaction;
DOI:10.1016/j.tetlet.2011.11.111