Technology Process of 2,2-diethyl-4,5-diphenyl-2H-imidazole
There total 4 articles about 2,2-diethyl-4,5-diphenyl-2H-imidazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium acetate; acetic acid;
for 2h;
Reflux;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/acscombsci.5b00107
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; magnesium sulfate heptahydrate; potassium permanganate / water; acetone / 1 h / 20 °C / Inert atmosphere; Schlenk technique
2: ammonium acetate; acetic acid / 2 h / Reflux; Inert atmosphere; Schlenk technique
With
potassium permanganate; magnesium sulfate heptahydrate; ammonium acetate; sodium hydrogencarbonate; acetic acid;
In
water; acetone;
DOI:10.1021/acscombsci.5b00107
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium dichloride; triphenylphosphine; pyrrolidine / water / 2 h / 120 °C / Inert atmosphere; Schlenk technique
2: sodium hydrogencarbonate; magnesium sulfate heptahydrate; potassium permanganate / water; acetone / 1 h / 20 °C / Inert atmosphere; Schlenk technique
3: ammonium acetate; acetic acid / 2 h / Reflux; Inert atmosphere; Schlenk technique
With
pyrrolidine; potassium permanganate; magnesium sulfate heptahydrate; ammonium acetate; sodium hydrogencarbonate; acetic acid; triphenylphosphine; palladium dichloride;
In
water; acetone;
1: |Sonogashira Cross-Coupling;
DOI:10.1021/acscombsci.5b00107
