3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

Base Information

Chemical Name:3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole
CAS No.:1361582-58-2
Molecular Formula:C₃₀H₂₈N₂O₄S₂
Molecular Weight:544.695
Hs Code.:

Synonyms:3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

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Chemical Property of 3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

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Technology Process of 3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

There total 5 articles about 3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 92988-08-4
trivinylboroxin

: C₂₈H₂₇BrN₂O₄S₂

: 1361582-58-2
3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; caesium carbonate; In 1,2-dimethoxyethane; at 85 ℃;
DOI:10.1002/chem.201501710

Reference yield: 82.0%

: 1361582-92-4
N-(3-bromobut-3-en-1-yl)-4-methyl-N-((1-tosyl-1H-indol-3-yl)ethynyl)benzenesulfonamide

: 2,4,6-trivinylcyclotriboroxane*pyridine complex

: 1361582-58-2
3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dimethoxyethane; water; for 16h; Reflux;
DOI:10.1002/chem.201102880

Reference yield:

: 80360-20-9
1-(phenylsulfonyl)indole-3-carbaldehyde

: 1361582-58-2
3-(5-phenyl-1-tosyl-2,3,4,5-tetrahydro-1H-indol-7-yl)-1-tosyl-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine / dichloromethane / 0.17 h / -20 °C

1.2: -78 - 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 °C

3.1: potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate / toluene / 16 h / 70 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; water / 1,2-dimethoxyethane / 85 °C

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; water; caesium carbonate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; toluene; 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/chem.201501710