3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

Base Information

Chemical Name:3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole
CAS No.:654679-55-7
Molecular Formula:C₃₃H₃₈O₆
Molecular Weight:530.661
Hs Code.:

Synonyms:3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

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Chemical Property of 3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

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Technology Process of 3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

There total 4 articles about 3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1458-98-6
2-methyl-3-bromo-1-propene

: 654679-49-9
3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

: 654679-55-7
3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2003.10.006

Reference yield:

: 16713-97-6
5-hydroxymethyl-3a-methoxymethyl-2,2-dimethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

: 654679-55-7
3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃N / CH₂Cl₂ / 6 h / 0 °C

2: 75 percent / NaH / dimethylformamide / 1 h / 20 °C

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2003.10.006

Reference yield:

: 17331-44-1
3a-methoxymethyl-2,2,7,7-tetramethyl-(3aS,4aS,8aR,8bS)-perhydro[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine

: 654679-55-7
3a-methoxymethyl-2,2-dimethyl-6-(2-methylallyloxy)-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / acetic acid / 12 h / 20 °C

2: 87 percent / Et₃N / CH₂Cl₂ / 6 h / 0 °C

3: 75 percent / NaH / dimethylformamide / 1 h / 20 °C

With sodium hydride; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2003.10.006