3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

Base Information

Chemical Name:3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol
CAS No.:654679-49-9
Molecular Formula:C₂₉H₃₂O₆
Molecular Weight:476.569
Hs Code.:

Synonyms:3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

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Chemical Property of 3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

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Technology Process of 3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

There total 3 articles about 3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 16713-97-6
5-hydroxymethyl-3a-methoxymethyl-2,2-dimethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

: 76-83-5
trityl chloride

: 654679-49-9
3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 6h;
DOI:10.1016/j.tetasy.2003.10.006

Reference yield:

: 17331-44-1
3a-methoxymethyl-2,2,7,7-tetramethyl-(3aS,4aS,8aR,8bS)-perhydro[1,3]dioxolo[4',5':4,5]furo[3,2-d][1,3]dioxine

: 654679-49-9
3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetic acid / 12 h / 20 °C

2: 87 percent / Et₃N / CH₂Cl₂ / 6 h / 0 °C

With acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.tetasy.2003.10.006

Reference yield:

: 17682-70-1
2,3:4,6-bis-O-isopropylidene-L-sorbose

: 654679-49-9
3a-methoxymethyl-2,2-dimethyl-5-trityloxymethyl-(3aS,5S,6R,6aS)-perhydrofuro[2,3-d][1,3]dioxol-6-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / KOH / dioxane / 5 h / 0 °C

2: 80 percent / acetic acid / 12 h / 20 °C

3: 87 percent / Et₃N / CH₂Cl₂ / 6 h / 0 °C

With potassium hydroxide; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.tetasy.2003.10.006