(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole
CAS No.:204057-84-1
Molecular Formula:C₂₂H₂₀F₁₃IO₄
Molecular Weight:722.282
Hs Code.:

Synonyms:(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

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Chemical Property of (3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

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Technology Process of (3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

There total 2 articles about (3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 355-43-1
n-perfluorohexyl iodide

: 19877-13-5
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranose

: 204057-84-1
(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: (3aR,5R,6S,6aR)-2,2-Dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-6-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoro-1-phenyl-heptyloxy)-tetrahydro-furo[2,3-d][1,3]dioxole

: meso-1,2-bis(5,6,7,8,9,10,11,12-octadeoxy-7,7,8,8,9,9,10,10,11,11,12,12,12-tridecafluoro-1,2-O-isopropylidene-α-D-xylododecanofuranos-3-yl)-1,2-diphenylethane

: 1,2-bis(5,6,7,8,9,10,11,12-octadeoxy-7,7,8,8,9,9,10,10,11,11,12,12,12-tridecafluoro-1,2-O-isopropylidene-α-D-xylododecanofuranos-3-yl)-1,2-diphenylethane

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In water; acetonitrile; at 20 ℃; for 1h; sonication;
DOI:10.1002/(SICI)1099-0690(199803)1998:3<531::AID-EJOC531>3.0.CO;2-E

Reference yield: 7.0%

: 355-43-1
n-perfluorohexyl iodide

: 19877-13-5
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranose

: 204057-92-1
(3aR,5R,6S,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 204057-84-1
(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In water; acetonitrile; at 20 ℃; for 24h;
DOI:10.1002/(SICI)1099-0690(199803)1998:3<531::AID-EJOC531>3.0.CO;2-E

Reference yield: 53.0%

: 204057-84-1
(3aR,5S,6R,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 204057-92-1
(3aR,5R,6S,6aR)-6-Benzyloxy-2,2-dimethyl-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 60 ℃; for 8h;
DOI:10.1002/(SICI)1099-0690(199803)1998:3<531::AID-EJOC531>3.0.CO;2-E