3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Base Information

Chemical Name:3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester
CAS No.:480446-64-8
Molecular Formula:C₂₂H₂₅N₃O₄
Molecular Weight:395.458
Hs Code.:

Synonyms:3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

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Chemical Property of 3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

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Technology Process of 3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

There total 3 articles about 3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 480446-63-7
(S)-3-(2-amino-phenylcarbamoyl)-2-t-butoxycarbonylaminopropionic acid benzyl ester

: 480446-64-8
3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Guidance literature:: With acetic acid; at 65 ℃; for 1h;
DOI:10.1021/jm020336e

Reference yield:

: 30925-18-9
2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

: 480446-64-8
3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NMM / dimethylformamide / 0.17 h / -20 °C

2: dimethylformamide / 4 h / -20 - 20 °C

3: 0.98 g / glacial AcOH / 1 h / 65 °C

With 4-methyl-morpholine; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm020336e

Reference yield:

: (S)-2-tert-Butoxycarbonylamino-4-isobutoxycarbonyloxy-4-oxo-butyric acid benzyl ester

: 480446-64-8
3-(1H-benzimidazol-2-yl)-2-tert-butoxycarbonylaminopropionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 4 h / -20 - 20 °C

2: 0.98 g / glacial AcOH / 1 h / 65 °C

With acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm020336e