N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

Base Information

Chemical Name:N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride
CAS No.:1353958-44-7
Molecular Formula:C₁₅H₈Cl₂F₃N₃O₂
Molecular Weight:390.149
Hs Code.:

Synonyms:N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

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Chemical Property of N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

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Technology Process of N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

There total 3 articles about N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1203256-54-5
3-nitro-2-[(trifluoromethyl)benzoyl] hydrazide

: 1353958-44-7
N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

Guidance literature:: With phosphorus pentachloride; In 1,2-dichloro-ethane; for 16h; Inert atmosphere; Reflux;

Reference yield:

: 618-94-0
3-nitrobenzoic acid hydrazide

: 1353958-44-7
N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: phosphorus pentachloride / 1,2-dichloro-ethane / 24 h / Inert atmosphere; Reflux

With phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja209325n

Reference yield:

: 329-15-7
4-trifluoromethyl-phenyl acetyl chloride

: 1353958-44-7
N'-(chloro(4-(trifluoromethyl)phenyl)methylene)-3-nitrobenzohydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: phosphorus pentachloride / 1,2-dichloro-ethane / 24 h / Inert atmosphere; Reflux

With phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja209325n