4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone

Base Information

• Chemical Name: 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone
• CAS No.: 301695-07-8
• Molecular Formula: C₁₉H₁₆ClFO₂S
• Molecular Weight: 362.852

Synonyms:4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone

Chemical Property of 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone

Chemical Property:

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Technology Process of 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone

There total 2 articles about 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-2-methylpropanoyl cyanide (55106-47-3) + 2-(3-chloro-phenyl)-1-(3-fluoro-4-methylsulfanyl-phenyl)-ethanone → 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone (301695-07-8)

Guidance literature:

2-(3-chloro-phenyl)-1-(3-fluoro-4-methylsulfanyl-phenyl)-ethanone; With sodium hydride; In tetrahydrofuran; at 0 ℃;

2-bromo-2-methylpropanoyl cyanide; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jm020545z

Reference yield:

→ 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone (301695-07-8)

Guidance literature:

Reference yield:

4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylthio)phenyl}-3(2H)-furanone (301695-07-8) → 4-(3-Chlorophenyl)-2,2-dimethyl-5-{3-fluoro-4-(methylsulfonyl)phenyl}-3(2H)-furanone

Guidance literature:

With oxone; In tetrahydrofuran; methanol; water; at 20 ℃;

DOI:10.1021/jm020545z

upstream raw materials:

2-bromo-2-methylpropanoyl cyanide

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