benzyl 4-amino-3-iodobenzoate

Base Information

Chemical Name:benzyl 4-amino-3-iodobenzoate
CAS No.:1325676-49-0
Molecular Formula:C₁₄H₁₂INO₂
Molecular Weight:353.159
Hs Code.:

Synonyms:benzyl 4-amino-3-iodobenzoate

Suppliers and Price of benzyl 4-amino-3-iodobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-amino-3-iodobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-amino-3-iodobenzoate

There total 4 articles about benzyl 4-amino-3-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1325676-47-8
benzyl 4-(bis(tert-butoxycarbonyl)amino)-3-iodobenzoate

: 1325676-49-0
benzyl 4-amino-3-iodobenzoate

Guidance literature:: benzyl 4-(bis(tert-butoxycarbonyl)amino)-3-iodobenzoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

With sodium hydroxide; In dichloromethane; water; pH=10 - 12;
DOI:10.1016/j.bmc.2011.05.036

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 1325676-49-0
benzyl 4-amino-3-iodobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine; silver sulfate / ethanol / 0.5 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

2.2: 12 h / 20 °C

2.3: pH 3 / Acidic aq. solution

3.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 24 h

4.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

4.2: pH 10 - 12

With dmap; iodine; silver sulfate; triethylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.036

Reference yield:

: 62875-84-7
3-iodobenzocaine

: 1325676-49-0
benzyl 4-amino-3-iodobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

1.2: 12 h / 20 °C

1.3: pH 3 / Acidic aq. solution

2.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 24 h

3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

3.2: pH 10 - 12

With dmap; triethylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.036