2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

Base Information

Chemical Name:2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether
CAS No.:730952-17-7
Molecular Formula:C₁₇H₁₇IO₂
Molecular Weight:380.225
Hs Code.:

Synonyms:2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

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Chemical Property of 2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

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Technology Process of 2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

There total 3 articles about 2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 781-03-3
isopentenyl tosylate

: 69358-20-9
2-iodo-4-phenoxyphenol

: 730952-17-7
2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

Guidance literature:: 2-iodo-4-phenoxyphenol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

isopentenyl tosylate; In N,N-dimethyl-formamide; at 25 ℃;
DOI:10.1021/ja047980y

Reference yield:

: 4-(methoxymethyloxy)phenyl phenyl ether

: 730952-17-7
2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 25 °C

1.2: 70 percent / I₂ / tetrahydrofuran; hexane / -78 °C

2.1: 100 percent / NaI; TMSCl / acetonitrile / 0 - 25 °C

3.1: NaH / dimethylformamide / 0 °C

3.2: 62 percent / dimethylformamide / 25 °C

With n-butyllithium; chloro-trimethyl-silane; sodium hydride; sodium iodide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja047980y

Reference yield:

: 730952-30-4
3-iodo-4-(methoxymethyloxy)phenyl phenyl ether

: 730952-17-7
2-iodo-4-phenoxyphenyl 3-methyl-3-butenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / NaI; TMSCl / acetonitrile / 0 - 25 °C

2.1: NaH / dimethylformamide / 0 °C

2.2: 62 percent / dimethylformamide / 25 °C

With chloro-trimethyl-silane; sodium hydride; sodium iodide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja047980y