4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

Base Information

Chemical Name:4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide
CAS No.:1422025-24-8
Molecular Formula:C₂₁H₂₉N₃O₄S
Molecular Weight:419.545
Hs Code.:

Synonyms:4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

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Chemical Property of 4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

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Technology Process of 4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

There total 6 articles about 4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1422027-03-9
4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxylic acid

: 1422025-24-8
4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

Guidance literature:: With ammonium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water;

Reference yield:

: 1057075-91-8
methyl 4-amino-adamantane-1-carboxylate hydrochloride

: 1422025-24-8
4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 12 h / 20 °C

2.2: pH 1 - 2

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonium hydroxide; benzotriazol-1-ol / water

With dmap; ammonium hydroxide; lithium hydroxide monohydrate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 105441-80-3
methyl 2-methyl-2-(phenylsulfonylamido)propionic acid

: 1422025-24-8
4-(2-methyl-2-(phenylsulfonamido)propanamido)adamantane-1-carboxyamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 12 h / 20 °C

2.2: pH 1 - 2

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ammonium hydroxide; benzotriazol-1-ol / water

With dmap; ammonium hydroxide; lithium hydroxide monohydrate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water;