2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

Base Information

Chemical Name:2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide
CAS No.:1196104-16-1
Molecular Formula:C₁₈H₂₃ClN₄O₄S
Molecular Weight:426.924
Hs Code.:

Synonyms:2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

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Chemical Property of 2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

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Technology Process of 2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

There total 3 articles about 2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1196104-04-7
3-tert-butyl-isoxazole-5-carboxamidine

: 1196104-02-5
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid hydrazide

: 1196104-16-1
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

Guidance literature:: With sodium methylate; In methanol; for 3h; Reflux;

Reference yield:

: 28361-38-8
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid

: 1196104-16-1
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

2.1: t-butoxycarbonylhydrazine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: 16 h / 20 °C

3.1: sodium methylate / methanol / 3 h / Reflux

With oxalyl dichloride; t-butoxycarbonylhydrazine; sodium methylate; N,N-dimethyl-formamide; In methanol; dichloromethane;

Reference yield:

: 1196103-81-7
2-(4-chlorobenzenesulfonyl)-2-methylpropionyl chloride

: 1196104-16-1
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-butoxycarbonylhydrazine / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 16 h / 20 °C

2.1: sodium methylate / methanol / 3 h / Reflux

With t-butoxycarbonylhydrazine; sodium methylate; In methanol; dichloromethane;