2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

Base Information

Chemical Name:2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole
CAS No.:1196103-47-5
Molecular Formula:C₁₈H₂₀ClN₃O₄S
Molecular Weight:409.894
Hs Code.:

Synonyms:2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

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Chemical Property of 2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

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Technology Process of 2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

There total 3 articles about 2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 1196104-16-1
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid [1-amino-1-(3-tert-butyl-isoxazol-5-yl)-methylidene]-hydrazide

: 1196103-47-5
2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

: 1196103-37-3
3-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl]-4H-[1,2,4]triazole

Guidance literature:: In o-xylene; at 140 ℃; for 1h;

Reference yield:

: 1196103-81-7
2-(4-chlorobenzenesulfonyl)-2-methylpropionyl chloride

: 1196103-47-5
2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

: 1196103-37-3
3-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl]-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-butoxycarbonylhydrazine / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 16 h / 20 °C

2.1: sodium methylate / methanol / 3 h / Reflux

3.1: o-xylene / 140 °C

With t-butoxycarbonylhydrazine; sodium methylate; In methanol; dichloromethane; o-xylene;

Reference yield:

: 1196104-02-5
2-(4-chloro-benzenesulfonyl)-2-methyl-propionic acid hydrazide

: 1196103-47-5
2-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl][1,3,4]oxadiazole

: 1196103-37-3
3-(3-tert-butyl-isoxazol-5-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl]-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 3 h / Reflux

2: o-xylene / 140 °C

With sodium methylate; In methanol; o-xylene;