O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid

Base Information

• Chemical Name: O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid
• CAS No.: 168139-24-0
• Molecular Formula: C₁₀H₁₂N₂O₃
• Molecular Weight: 208.217
• Mol file: 168139-24-0.mol

Synonyms:O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid

Chemical Property of O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid

There total 1 articles about O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

phenylglyoxylyl chloride (25726-04-9) + N-methoxylamine hydrochloride (593-56-6) → O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid (168139-24-0)

Guidance literature:

With pyridine; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/ja00122a018

Reference yield: 100.0%

O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid (168139-24-0) → C20H22N4O6

Guidance literature:

With nickel(IV) oxide; In tetrahydrofuran; at 25 ℃; for 12h;

DOI:10.1021/ja00122a018

Reference yield:

O-methyl-2-phenyl-2-methoxyiminoacetohydroxamic acid (168139-24-0) → methoxyimino-phenyl-acetic acid methyl ester (168139-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / NiO₂*H₂O / tetrahydrofuran / 12 h / 25 °C

2: 100 percent / 0.5 h / 100 - 160 °C / other N,N'-diacyl-N,N'-dialkoxyhydrazines

With nickel(IV) oxide; In tetrahydrofuran;

DOI:10.1021/ja00122a018

upstream raw materials:

phenylglyoxylyl chloride

N-methoxylamine hydrochloride

Downstream raw materials:

methoxyimino-phenyl-acetic acid methyl ester