C₃₀H₄₄O₁₁S

Base Information

Chemical Name:C₃₀H₄₄O₁₁S
CAS No.:568572-08-7
Molecular Formula:C₃₀H₄₄O₁₁S
Molecular Weight:612.739
Hs Code.:

C<sub>30</sub>H<sub>44</sub>O<sub>11</sub>S

Synonyms:C₃₀H₄₄O₁₁S

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Chemical Property of C₃₀H₄₄O₁₁S

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Technology Process of C₃₀H₄₄O₁₁S

There total 36 articles about C₃₀H₄₄O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 568572-05-4
C₂₃H₃₄O₈

: 568572-08-7
C₃₀H₄₄O₁₁S

Guidance literature:: Multi-step reaction with 8 steps

1: 88 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / 0.5 h / 0 °C

2: 83 percent / NaHCO₃; mCPBA / CH₂Cl₂ / 11.5 h / 20 °C

3: 81 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

4: 100 percent / Na[PhSeB(OEt)3] / ethanol / 0 - 20 °C

5: camphorsulfonic acid / CH₂Cl₂ / 4 h / 20 °C

6: L-Selectride / tetrahydrofuran / 0.75 h / -78 °C

7: 78.8 mg / LiAlH₄ / tetrahydrofuran / 0.67 h / 0 °C

8: 81 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; L-Selectride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; sodium phenylseleno(triethyl)borate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; 1: Luche reduction;
DOI:10.1021/ja042686r

Reference yield:

: 850656-91-6
C₁₈H₃₀O₇

: 568572-08-7
C₃₀H₄₄O₁₁S

Guidance literature:: Multi-step reaction with 12 steps

1: 0.972 g / pyridine / CH₂Cl₂ / 1.5 h / 20 °C

2: 81 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

3: LHMDS; Et₃N / tetrahydrofuran / 0.42 h / -78 °C

4: 587.4 mg / Pd(OAc)2 / acetonitrile / 15 h / 20 °C

5: 88 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / 0.5 h / 0 °C

6: 83 percent / NaHCO₃; mCPBA / CH₂Cl₂ / 11.5 h / 20 °C

7: 81 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

8: 100 percent / Na[PhSeB(OEt)3] / ethanol / 0 - 20 °C

9: camphorsulfonic acid / CH₂Cl₂ / 4 h / 20 °C

10: L-Selectride / tetrahydrofuran / 0.75 h / -78 °C

11: 78.8 mg / LiAlH₄ / tetrahydrofuran / 0.67 h / 0 °C

12: 81 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With pyridine; dmap; palladium diacetate; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; L-Selectride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; sodium phenylseleno(triethyl)borate; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile; 5: Luche reduction;
DOI:10.1021/ja042686r

Reference yield:

: 568571-87-9
(2S,3R,6S)-3-Benzyloxy-2-benzyloxymethyl-6-(4-methoxy-benzyloxy)-7-methylene-oxepane

: 568572-08-7
C₃₀H₄₄O₁₁S

Guidance literature:: Multi-step reaction with 21 steps

1.1: 9-BBN / tetrahydrofuran / 2.5 h / 20 °C

1.2: 9.46 g / Pd(PPh₃)4; aq. NaHCO₃ / dimethylformamide; tetrahydrofuran / 14 h / 50 °C

2.1: BH₃*SMe₂ / tetrahydrofuran / 4 h / 0 °C

2.2: 2.98 g / aq. H₂O₂; NaOH / tetrahydrofuran / 2.5 h / 20 °C

3.1: 96 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

4.1: 88 percent / DDQ; aq. phosphate buffer / CH₂Cl₂ / 1 h / 20 °C / pH 7

5.1: 92 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

6.1: 1.62 g / Zn(OTf)2 / CH₂Cl₂ / 25 h / 20 °C

7.1: 1.75 g / camphorsulfonic acid / CH₂Cl₂ / 2.5 h / 20 °C

8.1: 78 percent / Ph₃SnH; AIBN / toluene / 4 h / 110 °C

9.1: lithium 4,4'-di-tert-butylbiphenylide / tetrahydrofuran / 2 h / -78 °C

10.1: 0.972 g / pyridine / CH₂Cl₂ / 1.5 h / 20 °C

11.1: 81 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

12.1: LHMDS; Et₃N / tetrahydrofuran / 0.42 h / -78 °C

13.1: 587.4 mg / Pd(OAc)2 / acetonitrile / 15 h / 20 °C

14.1: 88 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / 0.5 h / 0 °C

15.1: 83 percent / NaHCO₃; mCPBA / CH₂Cl₂ / 11.5 h / 20 °C

16.1: 81 percent / N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate; 4A molecular sieves / CH₂Cl₂ / 1 h / 20 °C

17.1: 100 percent / Na[PhSeB(OEt)3] / ethanol / 0 - 20 °C

18.1: camphorsulfonic acid / CH₂Cl₂ / 4 h / 20 °C

19.1: L-Selectride / tetrahydrofuran / 0.75 h / -78 °C

20.1: 78.8 mg / LiAlH₄ / tetrahydrofuran / 0.67 h / 0 °C

21.1: 81 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; palladium diacetate; sodium tetrahydroborate; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; phosphate buffer; cerium(III) chloride; tetrapropylammonium perruthennate; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; 4,4'-di(tert-butyl)-[1,1-biphenyl]yllithium; 4 A molecular sieve; camphor-10-sulfonic acid; triphenylstannane; L-Selectride; zinc trifluoromethanesulfonate; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; sodium phenylseleno(triethyl)borate; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; acetonitrile; 1.2: Suzuki-Miyaura cross-coupling / 14.1: Luche reduction;
DOI:10.1021/ja042686r