5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

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Chemical Name:5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide
CAS No.:1309806-58-3
Molecular Formula:C₃₄H₄₁N₁₃O₅
Molecular Weight:711.784
Hs Code.:

5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

Synonyms:5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

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Chemical Property of 5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

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Technology Process of 5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

There total 4 articles about 5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1309806-56-1
N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)hept-6-ynamide

: 72200-24-9
N-(2-azidoethyl)-acetamide

: 1309806-58-3
5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; dimethyl sulfoxide; at 20 ℃; for 16h;
DOI:10.1016/j.bmcl.2010.11.082

Reference yield:

: 7-(3-(4-methoxyphenyl)propyl)-2-(2-furyl)pyrazolo[4,3-e]-1,2,4-triazolo[1,5-c]pyrimidine-5-amine

: 1309806-58-3
5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

Guidance literature:: Multi-step reaction with 5 steps

1: boron tribromide / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: caesium carbonate / methanol / 20 °C / Inert atmosphere

3: methanol / 36 h / 20 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

5: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 16 h / 20 °C

With copper(ll) sulfate pentahydrate; boron tribromide; caesium carbonate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.082

Reference yield:

: 1309806-51-6
methyl 2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetate

: 1309806-58-3
5-(1-(2-acetamidoethyl)-1H-1,2,3-triazol-4-yl)-N-(2-(2-(4-(3-(5-amino-2-(furan-2-yl)-7H-pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidin-7-yl)propyl)phenoxy)acetamido)ethyl)pentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 36 h / 20 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 16 h / 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.082