C₁₃H₉Cl₃F₃N₃O₃

Base Information

Chemical Name:C₁₃H₉Cl₃F₃N₃O₃
CAS No.:1435475-86-7
Molecular Formula:C₁₃H₉Cl₃F₃N₃O₃
Molecular Weight:418.587
Hs Code.:

C<sub>13</sub>H<sub>9</sub>Cl<sub>3</sub>F<sub>3</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₁₃H₉Cl₃F₃N₃O₃

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Chemical Property of C₁₃H₉Cl₃F₃N₃O₃

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Technology Process of C₁₃H₉Cl₃F₃N₃O₃

There total 5 articles about C₁₃H₉Cl₃F₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.8%

: 17647-70-0
3-amino-4-methylfurazan

: 1435476-01-9
C₁₀H₅Cl₄F₃O₂

: 1435475-86-7
C₁₃H₉Cl₃F₃N₃O₃

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 22 ℃; for 16.5h; Inert atmosphere;

Reference yield:

: 217479-60-2
(2,4,6-trichlorophenyl)methanol

: 1435475-86-7
C₁₃H₉Cl₃F₃N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: phosphorus tribromide / dichloromethane / 2 h / 0 - 22 °C

2.1: caesium carbonate; sodium iodide; N,N-dimethyl-formamide / 16 h / 22 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 1.17 h / -78 - 0 °C / Inert atmosphere

3.2: -78 - -50 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 22 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 16.5 h / -78 - 22 °C / Inert atmosphere

With n-butyllithium; oxalyl dichloride; phosphorus tribromide; caesium carbonate; diisopropylamine; N,N-dimethyl-formamide; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;

Reference yield:

: 50-43-1
2,4,6-trichlorobenzoic acid

: 1435475-86-7
C₁₃H₉Cl₃F₃N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-dimethyl sulfide complex / tetrahydrofuran / 22 °C / Inert atmosphere; Cooling with ice; Reflux

2.1: phosphorus tribromide / dichloromethane / 2 h / 0 - 22 °C

3.1: caesium carbonate; sodium iodide; N,N-dimethyl-formamide / 16 h / 22 °C

4.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 1.17 h / -78 - 0 °C / Inert atmosphere

4.2: -78 - -50 °C

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 22 °C

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 16.5 h / -78 - 22 °C / Inert atmosphere

With n-butyllithium; oxalyl dichloride; borane-dimethyl sulfide complex; phosphorus tribromide; caesium carbonate; diisopropylamine; N,N-dimethyl-formamide; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;