5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

Base Information

Chemical Name:5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile
CAS No.:1618698-45-5
Molecular Formula:C₂₅H₃₃NO₆SSi
Molecular Weight:503.692
Hs Code.:

Synonyms:5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

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Chemical Property of 5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

Chemical Property:

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Technology Process of 5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

There total 3 articles about 5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₃NO₅Si

: 124-63-0
methanesulfonyl chloride

: 1618698-45-5
5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

Guidance literature:: With pyridine; In water; at 0 - 20 ℃; for 6h;
DOI:10.1039/c4ob00931b

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1618698-45-5
5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodane; toluene-4-sulfonic acid / N,N-dimethyl-formamide

2: sodium hydrogencarbonate; hydroxylamine hydrochloride / ethanol; water / 72 h / 20 °C

3: pyridine / water / 6 h / 0 - 20 °C

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c4ob00931b

Reference yield:

: (3aS,6R,6aS)-6-((tert-butyldiphenylsilyloxy)methyl)-2,2-dimethyl-tetrahydrofuro[3,4-d]-[1,3]dioxol-4-ol

: 1618698-45-5
5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-O-methanesulfonyl-D-lyxononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; hydroxylamine hydrochloride / ethanol; water / 72 h / 20 °C

2: pyridine / water / 6 h / 0 - 20 °C

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol; water;
DOI:10.1039/c4ob00931b