Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester

Base Information

• Chemical Name: Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester
• CAS No.: 1028295-56-8
• Molecular Formula: C₂₉H₄₄N₂O₅S
• Molecular Weight: 532.745

Synonyms:Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester

Chemical Property of Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester

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Technology Process of Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester

There total 6 articles about Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester (1028295-56-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 30 g / NaOH / (C₈H₁₇)3NCH₃⁺Cl^- / toluene; H₂O / 65 h / Heating

2: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

3: triethylamine, DMAP / CH₂Cl₂ / 4 h / Ambient temperature

4: 74 percent / pyridine / tetrahydrofuran

5: triethylamine / tetrahydrofuran

With pyridine; dmap; sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; (C₈H₁₇)3NCH₃⁺Cl^-; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene;

DOI:10.1021/jm00104a002

Reference yield:

1-Bromotetradecane (112-71-0) → Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester (1028295-56-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 30 g / NaOH / (C₈H₁₇)3NCH₃⁺Cl^- / toluene; H₂O / 65 h / Heating

2: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

3: triethylamine, DMAP / CH₂Cl₂ / 4 h / Ambient temperature

4: 74 percent / pyridine / tetrahydrofuran

5: triethylamine / tetrahydrofuran

With pyridine; dmap; sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; (C₈H₁₇)3NCH₃⁺Cl^-; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene;

DOI:10.1021/jm00104a002

Reference yield:

1-nitro-4-(tetradecyloxy)benzene (94741-95-4) → Methanesulfonic acid 3-[3-(4-tetradecyloxy-phenyl)-ureido]-benzyl ester (1028295-56-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 25.7 g / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 2068.6 Torr

2: triethylamine, DMAP / CH₂Cl₂ / 4 h / Ambient temperature

3: 74 percent / pyridine / tetrahydrofuran

4: triethylamine / tetrahydrofuran

With pyridine; dmap; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;

DOI:10.1021/jm00104a002

upstream raw materials:

methanesulfonyl chloride

N-[3-(hydroxymethyl)phenyl]-N'-[4-(tetradecyloxy)phenyl]urea

4-nitro-phenol

1-Bromotetradecane

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