3-hydroxy-1-phenylbutyl phenyl sulphide

Base Information

Chemical Name:3-hydroxy-1-phenylbutyl phenyl sulphide
CAS No.:70769-84-5
Molecular Formula:C₁₆H₁₈OS
Molecular Weight:258.384
Hs Code.:

Synonyms:3-hydroxy-1-phenylbutyl phenyl sulphide

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Chemical Property of 3-hydroxy-1-phenylbutyl phenyl sulphide

Chemical Property:

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Technology Process of 3-hydroxy-1-phenylbutyl phenyl sulphide

There total 8 articles about 3-hydroxy-1-phenylbutyl phenyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 831-91-4
Benzyl phenyl sulfide

: 75-56-9,16033-71-9
methyloxirane

: 70769-84-5
3-hydroxy-1-phenylbutyl phenyl sulphide

Guidance literature:: Benzyl phenyl sulfide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

methyloxirane; In tetrahydrofuran; hexane; at 20 ℃; for 12h;
DOI:10.1002/jhet.5570370619

Reference yield:

: 70769-78-7
(Z)-4-Phenyl-4-phenylsulfanyl-but-3-en-2-one

: 70769-84-5
3-hydroxy-1-phenylbutyl phenyl sulphide

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; 1.) room temperature, 2 h, 2.) 30 min, reflux;
DOI:10.1039/P19810000934

Reference yield:

: 15745-68-3
(E)-1-phenyl-3-phenylsulfanyl-2-propen-1-one

: 70769-84-5
3-hydroxy-1-phenylbutyl phenyl sulphide

Guidance literature:: Multi-step reaction with 3 steps

1: 30.5 percent Chromat_. / NaBH₄ / methanol / 2 h / Ambient temperature

2: 75 percent / sodium methoxide / diethyl ether / 5 h / 0 °C

3: 100 percent Chromat_. / LiAlH₄ / diethyl ether / 1.) room temperature, 2 h, 2.) 30 min, reflux

With sodium tetrahydroborate; lithium aluminium tetrahydride; sodium methylate; In methanol; diethyl ether;
DOI:10.1039/P19810000934