N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

Base Information

Chemical Name:N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide
CAS No.:940943-43-1
Molecular Formula:C₁₇H₂₁N₃O₄S
Molecular Weight:363.437
Hs Code.:

Synonyms:N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

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Chemical Property of N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

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Technology Process of N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

There total 1 articles about N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 108-01-0
2-(N,N-dimethylamino)ethanol

: 940943-42-0
N-(5-acetyl-pyridin-2-yl)-4-iodo-benzenesulfonamide

: 940943-43-1
N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

Guidance literature:: 2-(N,N-dimethylamino)ethanol; N-(5-acetyl-pyridin-2-yl)-4-iodo-benzenesulfonamide; With caesium carbonate; copper(l) iodide; 1,10-Phenanthroline; at 120 ℃; for 16h;

With dipotassium hydrogenphosphate; potassium dihydrogenphosphate; In dichloromethane; water; pH=8.2;

Reference yield:

: 940943-43-1
N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide

: C₁₇H₂₀BrN₃O₄S

Guidance literature:: N-(5-Acetyl-pyridin-2-yl)-4-(2-dimethylamino-ethoxy)-benzenesulfonamide; With hydrogen bromide; pyrrolidone hydrotribromide; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; at 15 - 40 ℃; for 2h;

With dipotassium hydrogenphosphate; potassium dihydrogenphosphate; In tetrahydrofuran; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; pH=8.2;