Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate

Base Information

• Chemical Name: Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate
• CAS No.: 92532-13-3
• Molecular Formula: C₂₆H₃₄O₅
• Molecular Weight: 426.553

Synonyms:Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate

Chemical Property of Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate

Chemical Property:

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Technology Process of Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate

There total 8 articles about Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

3,4-dihydro-2H-pyran (110-87-2) + diethyl ether (60-29-7,927820-24-4) + methyl 3-[[3-(1-hydroxyhexyl)phenoxy]methyl]benzoate (92532-11-1) → Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate (92532-13-3)

Guidance literature:

toluene-4-sulfonic acid;

Reference yield: 67.0%

3,4-dihydro-2H-pyran (110-87-2) + methyl 3-[[3-(1-hydroxyhexyl)phenoxy]methyl]benzoate (92532-11-1) → Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate (92532-13-3)

Guidance literature:

With toluene-4-sulfonic acid; In diethyl ether; for 96h; Ambient temperature;

DOI:10.1021/jm00384a017

Reference yield:

1-methoxycarbonyl-3-methylbenzene (99-36-5) → Methyl-3-[[3-[1-(tetrahydro-2H-pyran-2-yloxy)hexyl]phenoxy]methyl]benzoate (92532-13-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Br₂ / CCl₄ / Heating; Irradiation

2: NaI, Cs₂CO₃ / acetone / 18 h / Heating

3: 67 percent / p-TsOH / diethyl ether / 96 h / Ambient temperature

With bromine; caesium carbonate; toluene-4-sulfonic acid; sodium iodide; In tetrachloromethane; diethyl ether; acetone;

DOI:10.1021/jm00384a017

upstream raw materials:

3,4-dihydro-2H-pyran

methyl 3-[[3-(1-hydroxyhexyl)phenoxy]methyl]benzoate

1-methoxycarbonyl-3-methylbenzene

1-(3-hydroxyphenyl)-1-hexanol

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