1-(3-hydroxyphenyl)-1-hexanol

Base Information

Chemical Name:1-(3-hydroxyphenyl)-1-hexanol
CAS No.:92532-21-3
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:194.274
Hs Code.:

Synonyms:1-(3-hydroxyphenyl)-1-hexanol

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Chemical Property of 1-(3-hydroxyphenyl)-1-hexanol

Chemical Property:

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Technology Process of 1-(3-hydroxyphenyl)-1-hexanol

There total 6 articles about 1-(3-hydroxyphenyl)-1-hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 147919-69-5
trans-3-(3-hex-2-enoyl)phenol

: 92532-21-3
1-(3-hydroxyphenyl)-1-hexanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 25 ℃; for 1h; under 760 Torr;
DOI:10.1021/jo00064a043

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 92532-21-3
1-(3-hydroxyphenyl)-1-hexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) lithium diisopropylamide / 1) THF, -78 deg C, 1 h, 2) THF, -78 deg C, 0.3 h

2: 80 percent / p-toluenesulfonic acid monohydrate, 3 Angstroem molecular sieves / toluene / 22 h / 40 °C

3: 98 percent / H₂ / 10percent Pd-C / ethanol / 1 h / 25 °C / 760 Torr

With 3 A molecular sieve; hydrogen; toluene-4-sulfonic acid; lithium diisopropyl amide; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1021/jo00064a043

Reference yield:

: 147919-68-4
3-(3-hydroxyhexanoyl)phenol

: 92532-21-3
1-(3-hydroxyphenyl)-1-hexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / p-toluenesulfonic acid monohydrate, 3 Angstroem molecular sieves / toluene / 22 h / 40 °C

2: 98 percent / H₂ / 10percent Pd-C / ethanol / 1 h / 25 °C / 760 Torr

With 3 A molecular sieve; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1021/jo00064a043