C₂₁H₂₉BO₃Si

Base Information

Chemical Name:C₂₁H₂₉BO₃Si
CAS No.:925231-60-3
Molecular Formula:C₂₁H₂₉BO₃Si
Molecular Weight:368.356
Hs Code.:

C<sub>21</sub>H<sub>29</sub>BO<sub>3</sub>Si

Synonyms:C₂₁H₂₉BO₃Si

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Chemical Property of C₂₁H₂₉BO₃Si

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Technology Process of C₂₁H₂₉BO₃Si

There total 5 articles about C₂₁H₂₉BO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92817-88-4
(2S)-3-{[tert-butyl(diphenyl)silyl]oxy}-2-methylpropanal

: 925231-60-3
C₂₁H₂₉BO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: Zn; Ph₃P / CH₂Cl₂ / 0.33 h / cooling

1.2: CH₂Cl₂ / 4 h / 20 °C

2.1: 5.61 g / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

3.1: BHBr₂*SMe₂ / CH₂Cl₂ / 2 h / 20 °C

3.2: 80 percent / H₂O / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

With n-butyllithium; dibromoborane dimethylsulfide; triphenylphosphine; zinc; In tetrahydrofuran; hexane; dichloromethane; 1.2: Corey-Fuchs homologation;
DOI:10.1002/anie.200603363

Reference yield:

: 95514-04-8
(R)-3-(tert-butyldiphenylsilyloxy)-2-methylpropan-1-ol

: 925231-60-3
C₂₁H₂₉BO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / Et₃N; SO₃; pyridine / CH₂Cl₂; dimethylsulfoxide / 1 h / 20 °C

2.1: Zn; Ph₃P / CH₂Cl₂ / 0.33 h / cooling

2.2: CH₂Cl₂ / 4 h / 20 °C

3.1: 5.61 g / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

4.1: BHBr₂*SMe₂ / CH₂Cl₂ / 2 h / 20 °C

4.2: 80 percent / H₂O / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

With pyridine; n-butyllithium; dibromoborane dimethylsulfide; sulfur trioxide; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; 2.2: Corey-Fuchs homologation;
DOI:10.1002/anie.200603363

Reference yield:

: 95514-03-7
(S)-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propionic acid methyl ester

: 925231-60-3
C₂₁H₂₉BO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 97 percent / LiBH₄ / tetrahydrofuran; diethyl ether / 24 h / 20 °C

2.1: 90 percent / Et₃N; SO₃; pyridine / CH₂Cl₂; dimethylsulfoxide / 1 h / 20 °C

3.1: Zn; Ph₃P / CH₂Cl₂ / 0.33 h / cooling

3.2: CH₂Cl₂ / 4 h / 20 °C

4.1: 5.61 g / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

5.1: BHBr₂*SMe₂ / CH₂Cl₂ / 2 h / 20 °C

5.2: 80 percent / H₂O / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

With pyridine; lithium borohydride; n-butyllithium; dibromoborane dimethylsulfide; sulfur trioxide; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; 3.2: Corey-Fuchs homologation;
DOI:10.1002/anie.200603363