5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

Base Information

Chemical Name:5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone
CAS No.:1187935-11-0
Molecular Formula:C₂₀H₂₁ClO₁₁
Molecular Weight:472.833
Hs Code.:

Synonyms:5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

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Chemical Property of 5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

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Technology Process of 5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

There total 3 articles about 5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1004782-77-7
5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-dimethoxybenzene

: 1187935-11-0
5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2011.07.024

Reference yield: 78.0%

: 1169858-32-5
5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-hydroquinone

: 1187935-11-0
5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

Guidance literature:: With silver(l) oxide; In chloroform; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2011.07.024

Reference yield:

: 210817-42-8
1,4-dimethoxy-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)benzene

: 1187935-11-0
5-chloro-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium nitrate; N-chloro-succinimide / acetonitrile / 3 h / 60 - 65 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C

With ammonium nitrate; N-chloro-succinimide; ammonium cerium (IV) nitrate; In water; acetonitrile;
DOI:10.1016/j.bmc.2011.07.024