dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

Base Information

Chemical Name:dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate
CAS No.:154921-12-7
Molecular Formula:C₁₄H₁₂I₃NO₇
Molecular Weight:686.965
Hs Code.:

Synonyms:dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

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Chemical Property of dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

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Technology Process of dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

There total 3 articles about dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-31-0
5-aminoisophthalic acid

: 154921-12-7
dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / aq. potassium iododichloride / H₂O / 18 h / 55 - 60 °C

2: 98 percent / methanol; diethyl ether / 1.) O deg C, 2 h, 2.) r.t., overnight

3: dioxane; toluene / 15 h / 60 °C

4: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

With potassium dichloroiodate; phenylmercuric acetate; In 1,4-dioxane; methanol; diethyl ether; water; toluene;
DOI:10.1021/jo00085a023

Reference yield:

: 35453-19-1
2,4,6-triiodo-5-aminoisophthalic acid

: 154921-12-7
dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / methanol; diethyl ether / 1.) O deg C, 2 h, 2.) r.t., overnight

2: dioxane; toluene / 15 h / 60 °C

3: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

phenylmercuric acetate; In 1,4-dioxane; methanol; diethyl ether; toluene;
DOI:10.1021/jo00085a023

Reference yield:

: 154921-11-6
dimethyl 5-amino-2,4,6-triiodo-1,3-benzenedicarboxylate

: 154921-12-7
dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane; toluene / 15 h / 60 °C

2: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

phenylmercuric acetate; In 1,4-dioxane; toluene;
DOI:10.1021/jo00085a023