Technology Process of dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate
There total 3 articles about dimethyl 2,4,6-triiodo-5-<<(oxiranylmethoxy)carbonyl>amino>-1,3-benzenedicarboxylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 74 percent / aq. potassium iododichloride / H2O / 18 h / 55 - 60 °C
2: 98 percent / methanol; diethyl ether / 1.) O deg C, 2 h, 2.) r.t., overnight
3: dioxane; toluene / 15 h / 60 °C
4: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
With
potassium dichloroiodate;
phenylmercuric acetate;
In
1,4-dioxane; methanol; diethyl ether; water; toluene;
DOI:10.1021/jo00085a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / methanol; diethyl ether / 1.) O deg C, 2 h, 2.) r.t., overnight
2: dioxane; toluene / 15 h / 60 °C
3: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
phenylmercuric acetate;
In
1,4-dioxane; methanol; diethyl ether; toluene;
DOI:10.1021/jo00085a023
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dioxane; toluene / 15 h / 60 °C
2: phenylmercuric acetate / dioxane / 4 h / Ambient temperature
phenylmercuric acetate;
In
1,4-dioxane; toluene;
DOI:10.1021/jo00085a023