N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

Base Information

Chemical Name:N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam
CAS No.:121195-35-5
Molecular Formula:C₃₅H₃₅NO₅
Molecular Weight:549.667
Hs Code.:

Synonyms:N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

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Chemical Property of N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

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Technology Process of N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

There total 4 articles about N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 121250-72-4
3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

: 100-44-7
benzyl chloride

: 121195-35-5
N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

Guidance literature:: With potassium carbonate; tetrabutylammomium bromide; In toluene; for 3h; Heating;
DOI:10.1016/0040-4020(89)80050-X

Reference yield:

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 121195-35-5
N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) acetonitrile, 16 deg C, 2 h; 2.) acetonitrile, -30 -> r.t.

2: 51 percent / K₂CO₃ / tetrabutylammonium bromide / toluene / 3 h / Heating

With potassium carbonate; tetrabutylammomium bromide; In toluene;
DOI:10.1016/0040-4020(89)80050-X

Reference yield:

: 100-39-0
benzyl bromide

: 121195-35-5
N-benzyl-3,4,6-tri-O-benzyl-2-carboxy-2-deoxy-α-D-galactohexopyranosylaminolactam

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium methoxide; 2.) KOH / 1.) MeOH; 2.) DMSO

2: 1.) acetonitrile, 16 deg C, 2 h; 2.) acetonitrile, -30 -> r.t.

3: 51 percent / K₂CO₃ / tetrabutylammonium bromide / toluene / 3 h / Heating

With potassium hydroxide; sodium methylate; potassium carbonate; tetrabutylammomium bromide; In toluene;
DOI:10.1016/0040-4020(89)80050-X