t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Base Information

Chemical Name:t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate
CAS No.:1334119-52-6
Molecular Formula:C₂₇H₂₇N₇O₄
Molecular Weight:513.556
Hs Code.:

Synonyms:t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

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Chemical Property of t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

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Technology Process of t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

There total 4 articles about t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-hydroxy-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

: 1334119-10-6
t-butyl benzoyl-(6-bromomethyl-pyridin-2-yl)-carbamate

: 1334119-52-6
t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: t-butyl benzoyl-(6-bromomethyl-pyridin-2-yl)-carbamate; With sodium hydroxide; at 20 - 25 ℃; for 0.5h;

N-hydroxy-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine; at 20 - 25 ℃; for 3.5h;

Reference yield:

: 1334119-08-2
t-butyl benzoyl-(6-methyl-pyridin-2-yl)-carbamate

: 1334119-52-6
t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2'-azobis(isobutyronitrile); 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol / chlorobenzene / 1 h / 90 °C

2.1: sodium hydroxide / 0.5 h / 20 - 25 °C

2.2: 3.5 h / 20 - 25 °C

With 2,2'-azobis(isobutyronitrile); 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; sodium hydroxide; In chlorobenzene;

Reference yield:

: 90101-22-7
2-(tert-butoxycarbonylamino)-6-picoline

: 1334119-52-6
t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; toluene / 0.83 h / 20 - 25 °C / Inert atmosphere

1.2: 0.42 h / 0 - 5 °C

2.1: 2,2'-azobis(isobutyronitrile); 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol / chlorobenzene / 1 h / 90 °C

3.1: sodium hydroxide / 0.5 h / 20 - 25 °C

3.2: 3.5 h / 20 - 25 °C

With 2,2'-azobis(isobutyronitrile); 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; sodium hydride; sodium hydroxide; In N,N-dimethyl-formamide; chlorobenzene; toluene;