Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester
CAS No.:500207-04-5
Molecular Formula:C20H23N7O3
Molecular Weight:409.448
Hs Code.:
Mol file:500207-04-5.mol

Synonyms:

Suppliers and Price of Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester

There total 10 articles about Carbamic acid, [6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]- 2-pyridinyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1334119-52-6
t-butyl benzoyl-{6-((Z)-(1-methyl-1H-5-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

Guidance literature:: With water; sodium hydroxide; In chlorobenzene; at 40 ℃; for 15h;

Reference yield:

: 888322-11-0
2-[bis(tert-butoxycarbonyl)amino]-6-(bromomethyl)pyridine

: N-hydroxy-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

: 1253511-94-2
t-butyl {6-([E]-(1-methyl-1H-S-tetrazolyl)phenylmethylene-aminooxymethyl)-2-pyridyl}carbamate

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In water; at 20 ℃; for 2h; Overall yield = 77.1 %; Overall yield = 6.1 g;

Reference yield:

: 1334119-10-6
t-butyl benzoyl-(6-bromomethyl-pyridin-2-yl)-carbamate

: 500207-04-5
tert-butyl N-[6-({[(Z)-[(1-methyl-1H-1,2,3,4-tetrazol-5-yl)(phenyl)methylidene]amino]oxy}methyl)pyridin-2-yl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 0.5 h / 20 - 25 °C

1.2: 3.5 h / 20 - 25 °C

2.1: sodium hydroxide / 15 h / 40 °C

With sodium hydroxide;