C₄₇H₅₆F₄N₄O₁₂

Base Information

Chemical Name:C₄₇H₅₆F₄N₄O₁₂
CAS No.:1419387-85-1
Molecular Formula:C₄₇H₅₆F₄N₄O₁₂
Molecular Weight:944.975
Hs Code.:

C<sub>47</sub>H<sub>56</sub>F<sub>4</sub>N<sub>4</sub>O<sub>12</sub>

Synonyms:C₄₇H₅₆F₄N₄O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₅₆F₄N₄O₁₂

Chemical Property:

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Technology Process of C₄₇H₅₆F₄N₄O₁₂

There total 17 articles about C₄₇H₅₆F₄N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13336-31-7
4-methoxylindanone

: 1419387-85-1
C₄₇H₅₆F₄N₄O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice

2.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

4.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

7.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

7.2: 4 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C / Cooling with ice

With pyridine; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; potassium tert-butylate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; toluene; acetonitrile;

Reference yield:

: 1419386-48-3
C₁₄H₁₆O₂

: 1419387-85-1
C₄₇H₅₆F₄N₄O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

3.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

4.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

6.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

6.2: 4 h / 0 °C

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C / Cooling with ice

With pyridine; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1419386-97-2
C₁₄H₁₈O

: 1419387-85-1
C₄₇H₅₆F₄N₄O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

2.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

3.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

5.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

5.2: 4 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C / Cooling with ice

With pyridine; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;