[(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene

Base Information

Chemical Name:[(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene
CAS No.:69967-85-7
Molecular Formula:C₁₆H₁₅Cl
Molecular Weight:242.748
Hs Code.:
NSC Number:168888
DSSTox Substance ID:DTXSID90421023
Wikidata:Q82232364

Synonyms:NSC168888;69967-85-7;SCHEMBL18874673;DTXSID90421023;NSC-168888

Suppliers and Price of [(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of [(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:242.0862282
Heavy Atom Count:17
Complexity:255

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=C(C1=CC=CC=C1)Cl)C2=CC=CC=C2
Isomeric SMILES:CC/C(=C(\C1=CC=CC=C1)/Cl)/C2=CC=CC=C2

Technology Process of [(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene

There total 5 articles about [(Z)-1-chloro-1-phenylbut-1-en-2-yl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773-47-7
dimethyl benzylphosphonate

: 69967-85-7
(E)-1-Chloro-1,2-diphenyl-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / chlorination

2: 1.) tert-butyllithium / 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux

With tert.-butyl lithium;
DOI:10.1021/jo00164a036

Reference yield:

: 100-44-7
benzyl chloride

: 69967-85-7
(E)-1-Chloro-1,2-diphenyl-1-butene

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / 20 h / Heating

2: 96 percent / chlorination

3: 1.) tert-butyllithium / 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux

With tert.-butyl lithium;
DOI:10.1021/jo00164a036

Reference yield:

: 16965-75-6
Dimethyl 1-Chloro-1-phenylmethanephosphonate

: 93-55-0
1-phenyl-propan-1-one

: 69967-85-7
(E)-1-Chloro-1,2-diphenyl-1-butene

: 69967-86-8
(Z)-1-Chloro-1,2-diphenyl-1-butene

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux;
DOI:10.1021/jo00164a036