(2RS,3RS)-2--1-methylpropyl benzoate

Base Information

Chemical Name:(2RS,3RS)-2--1-methylpropyl benzoate
CAS No.:114431-75-3
Molecular Formula:C₁₉H₂₄O₂Si
Molecular Weight:312.484
Hs Code.:

(2RS,3RS)-2-<dimethyl(phenyl)silyl>-1-methylpropyl benzoate

Synonyms:(2RS,3RS)-2--1-methylpropyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3RS)-2--1-methylpropyl benzoate

Chemical Property:

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Technology Process of (2RS,3RS)-2--1-methylpropyl benzoate

There total 3 articles about (2RS,3RS)-2--1-methylpropyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 93-97-0
benzoic acid anhydride

: (2RS,3RS)-3-dimethyl(phenyl)silylbutan-2-ol

: 114431-75-3
(2RS,3RS)-2--1-methylpropyl benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 75589-94-5
(E)-dimethyl(phenyl)(prop-1-en-1-yl)silane

: 114431-75-3
(2RS,3RS)-2--1-methylpropyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / chloroperbenzoic acid, Na₂HPO₄ / CH₂Cl₂ / 20 h / Ambient temperature

2: 93 percent / CuI / diethyl ether / 1.) -78 deg C -> -40 deg C, 2.) -40 deg C -> room temperature

3: 89 percent / Et₃N, DMAP / CH₂Cl₂ / 12 h / Ambient temperature

With dmap; disodium hydrogenphosphate; copper(l) iodide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

Reference yield:

: (RS,RS)-1-dimethyl(phenyl)silyl-1,2-epoxypropane

: 114431-75-3
(2RS,3RS)-2--1-methylpropyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / CuI / diethyl ether / 1.) -78 deg C -> -40 deg C, 2.) -40 deg C -> room temperature

2: 89 percent / Et₃N, DMAP / CH₂Cl₂ / 12 h / Ambient temperature

With dmap; copper(l) iodide; triethylamine; In diethyl ether; dichloromethane;