N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

Base Information

Chemical Name:N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine
CAS No.:1384260-59-6
Molecular Formula:C₂₇H₂₀Cl₄N₄O₇
Molecular Weight:654.29
Hs Code.:

N<sub>4</sub>-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

Synonyms:N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

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Chemical Property of N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

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Technology Process of N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

There total 3 articles about N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1571-13-7
3,4,5,6-tetrachlorophthalimide

: 39946-94-6,98807-30-8
4-N-benzoyl-2',3'-O-isopropylidenecytidine

: 1384260-59-6
N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 15h; Reflux;
DOI:10.1016/j.tetlet.2012.05.055

Reference yield:

: 98-88-4
benzoyl chloride

: 1384260-59-6
N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; chloro-trimethyl-silane

2: toluene-4-sulfonic acid / water; acetone / 24 h / Reflux

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 15 h / Reflux

With pyridine; chloro-trimethyl-silane; di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; water; acetone; 3: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2012.05.055

Reference yield:

: 65-46-3
CYTIDINE

: 1384260-59-6
N₄-benzoyl-5'-tetrachlorophthalimido-2',3'-O-isopropylidene-5'-deoxycytidine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; chloro-trimethyl-silane

2: toluene-4-sulfonic acid / water; acetone / 24 h / Reflux

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 15 h / Reflux

With pyridine; chloro-trimethyl-silane; di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; water; acetone; 3: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2012.05.055