(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

Base Information

Chemical Name:(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate
CAS No.:1313878-07-7
Molecular Formula:C₁₇H₂₃BO₄
Molecular Weight:302.178
Hs Code.:

Synonyms:(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

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Technology Process of (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

There total 5 articles about (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 167896-49-3
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-ol

: 108-24-7
acetic anhydride

: 1313878-07-7
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1055/s-0040-1707468

Reference yield:

: 1138162-59-0
C₁₈H₂₉BO₃Si

: 1313878-07-7
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water / 0.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-0040-1707468

Reference yield:

: 4187-87-5
1-Phenyl-2-propyn-1-ol

: 1313878-07-7
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: 12 h / 150 °C

3: hydrogenchloride / tetrahydrofuran; water / 0.5 h / 0 - 20 °C / Inert atmosphere

4: triethylamine; dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-0040-1707468