(N-tert-butyl-α-phenylnitrone) azidyl adduct

Base Information

• Chemical Name: (N-tert-butyl-α-phenylnitrone) azidyl adduct
• CAS No.: 58200-47-8
• Molecular Formula: C₁₁H₁₅N₄O
• Molecular Weight: 219.266
• Mol file: 58200-47-8.mol

Synonyms:(N-tert-butyl-α-phenylnitrone) azidyl adduct

Chemical Property of (N-tert-butyl-α-phenylnitrone) azidyl adduct

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (N-tert-butyl-α-phenylnitrone) azidyl adduct

There total 8 articles about (N-tert-butyl-α-phenylnitrone) azidyl adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium azide + N-tert-butyl-α-phenylnitrone (3376-24-7,68315-30-0) + titanium(IV) oxide → di-tert-butyl nitroxide (2406-25-9,44871-19-4) + (N-tert-butyl-α-phenylnitrone) azidyl adduct (58200-47-8)

Guidance literature:

In methanol; water; Irradiation (UV/VIS); Irradn. of a TiO2 suspn. in water/methanol containing sodium azide and PBN.; Monitored by ESR.;

Reference yield:

sodium azide + 5,10,15,20-tetrakis(4-sulfonatophenyl)porphyrinatoiron(III) (60489-11-4) + N-tert-butyl-α-phenylnitrone (3376-24-7,68315-30-0) → di-tert-butyl nitroxide (2406-25-9,44871-19-4) + (N-tert-butyl-α-phenylnitrone) azidyl adduct (58200-47-8)

Guidance literature:

In ethanol; water; Irradiation (UV/VIS); Irradn. of a deaerated soln. of Fe(III)TPPS4 in ethanol/water containing NaN3 and PBN.; Monitored by ESR.;

Reference yield:

N-tert-butyl-α-phenylnitrone (3376-24-7,68315-30-0) → di-tert-butyl nitroxide (2406-25-9,44871-19-4) + (N-tert-butyl-α-phenylnitrone) azidyl adduct (58200-47-8)

Guidance literature:

With sodium azide; titanium(IV) oxide; In water; Product distribution; Irradiation; dependence of the time of irradiation, N^-3 concentration, different pH values and solvents; with esr detected;

upstream raw materials:

t-butylnitrite

di-tert-butoxydiazene

benzyl azide

(Z)-N-benzylidene-2-methylpropan-2-amine oxide

Downstream raw materials:

t-butylnitrite