8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane

Base Information

• Chemical Name: 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane
• CAS No.: 915708-14-4
• Molecular Formula: C₂₈H₄₁ClO₅
• Molecular Weight: 493.084

Synonyms:8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane

Chemical Property of 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane

Chemical Property:

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• Pictogram(s):  
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Technology Process of 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane

There total 2 articles about 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.01,5]undecan-8-ol (915708-13-3) → 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.01,5]undecane (915708-14-4)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; thionyl chloride; at 0 - 20 ℃;

DOI:10.1002/anie.200602056

Reference yield:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.01,5]undecan-8-one (915708-12-2) → 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.01,5]undecane (915708-14-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / -20 °C

2: SOCl₂; DMPU / 0 - 20 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; thionyl chloride; In tetrahydrofuran;

DOI:10.1002/anie.200602056

Reference yield:

8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.01,5]undecane (915708-14-4) → 3-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8a-(4-methoxy-benzyloxymethyl)-6-methyl-2,3,4,5,8,8a-hexahydro-1H-azulen-3a-ol (915708-15-5)

Guidance literature:

With sodium; In diethyl ether; for 12h; Heating;

DOI:10.1002/anie.200602056

upstream raw materials:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-ol

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one

Downstream raw materials:

3-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8a-(4-methoxy-benzyloxymethyl)-6-methyl-2,3,4,5,8,8a-hexahydro-1H-azulen-3a-ol

deacetylpseudolaric acid A

pseudolaric acid A

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