Technology Process of 3-benzyl-1,2,4,5-tetramethoxybenzene
There total 4 articles about 3-benzyl-1,2,4,5-tetramethoxybenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; palladium diacetate; triphenylphosphine;
In
toluene;
at 100 ℃;
for 16h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2013.06.039
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide; sulfuric acid / methanol / 2 h / 20 °C
2: potassium carbonate / acetone / 18 h / 65 °C
3: hydrogen bromide / acetic acid / 6 h / 55 °C
4: potassium phosphate; palladium diacetate; triphenylphosphine / toluene / 16 h / 100 °C / Inert atmosphere
With
potassium phosphate; sulfuric acid; hydrogen bromide; dihydrogen peroxide; palladium diacetate; potassium carbonate; triphenylphosphine;
In
methanol; acetic acid; acetone; toluene;
DOI:10.1016/j.ejmech.2013.06.039
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / 18 h / 65 °C
2: hydrogen bromide / acetic acid / 6 h / 55 °C
3: potassium phosphate; palladium diacetate; triphenylphosphine / toluene / 16 h / 100 °C / Inert atmosphere
With
potassium phosphate; hydrogen bromide; palladium diacetate; potassium carbonate; triphenylphosphine;
In
acetic acid; acetone; toluene;
DOI:10.1016/j.ejmech.2013.06.039
