benzyl allyl-(3-oxobutyl)carbamane

Base Information

• Chemical Name: benzyl allyl-(3-oxobutyl)carbamane
• CAS No.: 514848-49-8
• Molecular Formula: C₁₅H₁₉NO₃
• Molecular Weight: 261.321
• Mol file: 514848-49-8.mol

Synonyms:benzyl allyl-(3-oxobutyl)carbamane

Chemical Property of benzyl allyl-(3-oxobutyl)carbamane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzyl allyl-(3-oxobutyl)carbamane

There total 1 articles about benzyl allyl-(3-oxobutyl)carbamane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl vinyl ketone (78-94-4,25038-87-3) + benzyl chloroformate (501-53-1,94274-21-2) + 1-amino-2-propene (107-11-9,30551-89-4) → benzyl allyl-(3-oxobutyl)carbamane (514848-49-8)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran;

DOI:10.1021/ol0706004

Reference yield:

benzyl allyl-(3-oxobutyl)carbamane (514848-49-8) → C15H21NO5

Guidance literature:

With osmium(VIII) oxide; N-methyl-2-indolinone; In water; acetone; tert-butyl alcohol; at 0 - 20 ℃; for 8h;

DOI:10.1021/ol0706004

Reference yield:

benzyl allyl-(3-oxobutyl)carbamane (514848-49-8) → benzyl (3-oxobutyl)-(2-oxoethyl)carbamate (944413-17-6)

Guidance literature:

Multi-step reaction with 2 steps

1: OsO₄; NMO / acetone; H₂O; 2-methyl-propan-2-ol / 8 h / 0 - 20 °C

2: NaIO₄ / aq. phosphate buffer; tetrahydrofuran / 2 h / 0 - 20 °C / pH 7

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; In tetrahydrofuran; phosphate buffer; water; acetone; tert-butyl alcohol;

DOI:10.1021/ol0706004

upstream raw materials:

methyl vinyl ketone

benzyl chloroformate

1-amino-2-propene

Downstream raw materials:

benzyl (3-oxobutyl)-(2-oxoethyl)carbamate

Refernces